Nano nickel [1,2,4]-triazole-3-thiones complex: Design, sonochemical synthesis, and antimicrobial evaluation
Soliman Farag Saad, Paula; Magdy M. Hemdan; El-Hag, Amira;
Abstract
A series of new 1,2,4-triazole-3-thiones were synthesized by calm, benign,
no risk, eco-friendly, and energy efficient sequential reaction methodology
like grinding and ultrasonic (US). In addition, 1,2,4-triazoles were prepared
under conventional method and comparative study was done. The synthesized
1,2,4-triazoles were complexed with Ni(II) to produce nanoparticles complexes
(NPC's) with average particle size vary from 55 to 100 nm (using scanning electron
microscope technique) with good yields via both US and conventional
techniques. X-ray diffraction technique and spectra analysis techniques were
used to confirm the square planer geometry of the synthesized NPC's. Antimicrobial
activity of the prepared 1,2,4-triazoles and their nickel complexes were
studied which evaluated a high activity with complexes instead their triazoles
no risk, eco-friendly, and energy efficient sequential reaction methodology
like grinding and ultrasonic (US). In addition, 1,2,4-triazoles were prepared
under conventional method and comparative study was done. The synthesized
1,2,4-triazoles were complexed with Ni(II) to produce nanoparticles complexes
(NPC's) with average particle size vary from 55 to 100 nm (using scanning electron
microscope technique) with good yields via both US and conventional
techniques. X-ray diffraction technique and spectra analysis techniques were
used to confirm the square planer geometry of the synthesized NPC's. Antimicrobial
activity of the prepared 1,2,4-triazoles and their nickel complexes were
studied which evaluated a high activity with complexes instead their triazoles
Other data
Title | Nano nickel [1,2,4]-triazole-3-thiones complex: Design, sonochemical synthesis, and antimicrobial evaluation | Authors | Soliman Farag Saad, Paula ; Magdy M. Hemdan; El-Hag, Amira | Issue Date | 8-Jun-2020 | Publisher | wily | Journal | JOURNAL OF HETEROCYCLIC CHEMISTRY | Volume | 57 | Issue | 9 | Start page | 3428 | End page | 3441 | DOI | 10.1002/jhet.4063 |
Attached Files
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Paula J of Heterocyclic 2020 نشر دولى 04012021.pdf | 3 MB | Adobe PDF | Request a copy |
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